Epoxy Prepreg

Why Choose Us

Large Factory Area
The resin factory is located in Shanghai, with more than 15 acres of factory buildings and land reserves, employing more than 300 technical personnel and more than 500 employees. The DFPA factory is located in Northeast China, with 20 acres of factory buildings and land reserves, more than 200 technicians and more than 300 employees.

 

Quality Assurance
We have a complete quality management system and automated production equipment. The entire production process operates under the ISO9001 quality management system. And we have GB/T24001-2016//ISO14001:2015, GB/T19001-2016//ISO9001:2015, GB/T28001-2011 //OHSAS18001:2007 and GB/T23331-2012//ISO50001:2011//RB/ T 114-2014 certificates.

 

Rich Products
Our company mainly produces epoxy resin for coatings, epoxy resin for electronics, epoxy resin adhesives, epoxy resin for wind power generation, pesticide intermediates, etc. And epoxy resin is widely used in various types of coatings, electronic packaging, adhesives, wind power composite materials and other fields.

 

Rich Experience
Our company was established in 1999 and has been working in the field of resin chemicals for more than 20 years. Currently, it can produce more than 5,000 tons of new pesticide intermediates every year; and the company has the most advanced laboratories.

 
What is Epoxy Prepreg?

Epoxy prepreg is a composite material consisting of reinforcing fibers pre-impregnated with an epoxy resin. The term "prepreg" comes from the process of "preparing" the reinforcement by partially curing the resin so that it is tacky but not fully set. This allows the prepreg to be cut, shaped, and laid up into a mold or laminate with precision and ease.

 

Advantages of Epoxy Prepreg
 

Peerless Mechanical Performance: Its simple, an optimized fiber to resin ratio provides the best mechanical properties in the lightest weight for a composite design or fabrication. Prepregs provide just that.

 

Process Robustness: Prepregs provide a much cleaner and easier processing from ply cut to demold. Clean and easy ply cut of prepregs result in accurately ply shapes that are then easily laid up into mold surfaces. No longer is there a sticky mess of resin coming from your gloves while trying to layup large plys of complex surfaces while handling brushes or squeegees. No longer is there even resin mixing, no working times down to the min to worry about, no complicated system of resin feed lines, no worrying if the spray adhesive will affect a part’s surface finish. The list is nearly endless with it comes to reducing man hours, touch times, and efficiency of composite fabrication processes.

 

Unmatched Repeatability & Uniformity: Process robustness and consistency go together in effectively fabricating repeatable high-quality parts. Prepregs mitigate process variation as it is optimized with features such as tack, cured ply thickness, and a debulking capability that make even the most complicated laminates easier. Prepregs are consistent, simply pull the backing from the cut plys and lay it into the mold, conforming the ply to the mold as needed. Once the layup is complete, the bagging and curing process is much less complicated than that of an infusion process.

 

Co-cure > Secondary Cure: One large advantage to using prepregs in composites lies in the ability to co-cure many aspects of a composite laminate in one shot. Co-curing adds to the high-performance capability because co-cured laminates share stronger bonds than that of secondary bonds. Products such as film adhesives allow core bonded composites to be made in one cure run with the prepreg fabric layers. In addition, large core pieces can be joined via syntactic films, lighting strike protection can be added to the surface of conductive materials and other film adhesives can be used to provide a higher quality surface finish. In short, many of vacuum infusion and traditional layup shortcomings are made simple using prepreg products.

 

Basic knowledge of Epoxy Prepreg

 

 

“Prepreg” is broad terminology in composite fabrication used for describing fabrics that are pre-impregnated with a fully curable, mixed resin system during manufacture. Prepregs are often regarded as the most advanced system of composite fabrication. By simply adding a mold, heat, and pressure, use of prepreg fabrics virtually eliminate process variation found in traditional layups or vacuum infusion processes. As a result, prepregs have revolutionized composite fabrication as we know it and are most often chosen for achieving the highest performance characteristics in fiber reinforced structures.

Carbon Fiber, Kevlar, and Fiberglass are the most used fabrics in Prepreg reinforced composites. Historically, Prepregs most popular use was aerospace and aviation applications. As technology has advanced, prepreg fabrics are now more affordable and have found additional market value in high performance applications of automobile manufacture and racing, boating, sporting goods, and even construction.

Prepregs are a calculated combination of reinforcing fabric paired with a semi-cured resin system that is most often Epoxy based. This matrix, a calculated weight ratio for prepregs is responsible for achieving the light-weight performance characteristics in a composite laminate. Prepregs can achieve a ratio as low as 35% resin, which is unheard of with any other layup methods.

Basic prepreg selection is based on characteristics such as fiber, tow size, and weave selection, all of which are similar features to that of traditional fabrics. Prepregs will often come with a defined “cured ply thickness” and density in addition to providing the precise fiber to resin ratio. The resin added to the fabric also doubles to make layup processes much more effective as they carry a tack in making layup more effective.

Because resins in prepregs flow and cure in a different manner than infusion or traditional layup methods, they require pressure and heat for cure. Once a layup of prepreg fabrics has been completed, it must then be cured by a combination of heat and vacuum. This is often referred to as a cure cycle performed inside an oven or an autoclave. For complex laminates, an autoclave, like a large pressure cooker, provides pressure far beyond vacuum alone. General epoxy prepregs are commonly cured between 250F and 350F.

 

Materials Used for Epoxy Flooring

 

How do Epoxy Prepreg work?

Fibre Glast prepreg fabric will be shipped to you sandwiched between two layers of backing cloth. This cloth keeps the prepreg from sticking together. Peeling off the protective backing is easy, and the material is immediately ready for layup.

To completely cure the prepreg, heat and pressure are required. Although the pressure could be achieved using a press, the more typical method is vacuum bagging. After the part is laid up, it must be vacuum bagged with all of the usual elements – a bag to hold the vacuum, peel ply so the bag does not stick to the part, and bleeder/breather cloth to absorb the excess resin.

The ideal curing environment would be an autoclave which has both temperature and pressure controls, although prepregs are commonly cured otherwise.

The heat requirements generally require an oven in order to control temperature ramp up, ramp down, and to sustain a controlled, uniform temperature for the recommended duration. Ovens used for curing composites should never be used for cooking food as there will be contaminants released.

Heat lamps can be used to create enough heat, but the trial and error associated with controlling the temperature will cause problems.

 

How to use Epoxy Prepreg

 

 

First, prepare your mold as you usually would. To obtain a glossy finished part, it is necessary to have a flawless mold which has been waxed and coated with PVA. The prepreg is supplied between two backing sheets which need to be peeled away before laying the fabric into the mold. Because the prepreg surface is very tacky, it is necessary to place the material carefully into the mold. Unlike a dry fabric in a hand lamination, you cannot reposition the prepreg without fixing your mold release. Repositioning will pull up the PVA. You can continue to place layers on top of each other up to a total thickness of one-quarter inch at a single time.

The prepreg is partially cured which means that it is in B-Stage. It can be trimmed, pleated, and formed using a knife or a pair of scissors. The prepreg handles very easily and because of its tackiness, it will lay tightly into your mold. You might still have relief cuts or pleats to contend with just like you would with a dry fabric.

After placing the layers in the mold, the prepreg must be compressed to allow bonding, to remove any trapped air between the layers and to squeeze out any excess resin. Although there will be very little excess, the resin will naturally become thinner as the temperature is raised and there will be resin flow prior to a full cure of the resin.

The needed compression can be accomplished using a press but unless the part is perfectly flat, a press is not an option. Consequently, the part is generally vacuum bagged.

With prepreg fabric, there is a benefit in having plenty of time to build your bag and get the part ready for the oven. You are not fighting the natural pot life of the resin. However, the more layers you have laid, the more likely that there will be air trapped between the layers. You should really have perfected your vacuum bagging technique before laying multiple layers of prepreg for a single curing.

A big advantage of prepregs is that after curing and cooling, additional layers can be laid onto the part without scuffing or additional surface preparation. Again, up to one-quarter inch can be laid at a single time with the same consideration of not trapping air between layers.

After the layup is complete, the vacuum bag is built and sealed, and you are ready to pull vacuum and begin the heat cycle. There are three recommended cure cycles for Fibre Glast prepregs and all will produce similar properties.

All curing cycles begin with a temperature ramp up and end with a ramp down. The difference is the target temperature and the amount of time required for a complete cure. Always ramp up at a rate of no more than 5°F per minute until the target temperature is attained. Maintain the target temperature throughout the cure cycle and then ramp down at a rate of less than 5°F per minute to at least 150°F before removing from the oven.

Let the part cool to room temperature, remove the vacuum bagging materials, and release the part from the mold. Your part should be fully cured and can be put into immediate service.

There are several considerations when determining the amount of time and heat to use. First, if you are not in a hurry, plan to go low on temperature and long on time. You can leave the part in the heat up to 24 hours without any risk of damage to the part. You cannot "overcook" your prepreg. You can, however, "undercook" it.

Second, when determining your temperature and cure cycle, consider the mass and conductivity of your mold. If it is thin metal (low mass and conductive), it will heat up quickly and not interfere with the curing cycle. If it is thick fiberglass (high mass and not conductive), it will take a while to heat up and you will want to be on the conservative side of time and temperature.

 

There are several advantages to using a Epoxy Prepreg rather than using traditional hand layup
1

Maximum strength properties. In a hand layup, it is difficult to achieve 50% resin content. This means that the finished laminate weight is 50% fabric and 50% resin. Typical hand laminates, even when vacuum bagged, end up with a significant amount of excess resin. Excess resin increases brittleness and reduces overall properties. On the other hand, most prepregs contain around 35% resin. This is ideal for maximum cured properties and generally impossible to achieve in normal hand lamination.

2

Part uniformity and repeatability. Without the pitfalls of human lamination techniques, there will be neither resin-rich areas nor dry spots. Thickness will be uniform and every part that comes out of the mold has a theoretical likelihood of being identical. There is still a margin for error in vacuum bagging techniques, handling, etc., but prepregs reduce these problems significantly.

3

Less mess and less waste. Prepregs will bleed excess resin during the curing process but all of the excesses of hand layup – cups of resin, messy rollers, drips – are no longer a problem. Plus, Fibre Glast prepregs are handled at room temperature so you are not fighting a clock trying to avoid your resin setting up before you are ready.

4

Less curing time. After the heat curing cycle is completed, the part is ready for service. You do not have to wait the standard 48 hours to allow a full cure as in a typical hand lamination.

5

Better cosmetics. Mold preparation and mold release is still required and will directly affect the cosmetics of the part just like a hand laminate. However, Fibre Glast prepregs virtually eliminate air bubbles and a smooth, glossy surface is more easily attainable.

 

Types of Epoxy Prepreg Manufacturing

There are two main types of the Epoxy Prepreg process, as described here:
Solvent Dip
In the solvent dip prepreg method, the resin is dissolved in a solvent bath and the reinforcing fabric is dipped in the resin solution. The solvent is then evaporated off the prepreg using a drying oven. Only fabric prepregs can be produced using this process.

Hot Melt
In the hot melt prepreg method, the resin film is cast on a fibre-based carrier material, before both materials are passed between heated rollers. This transfers the resin to the carrier material and forces the resin to impregnate the carrier’s fibres.

 

Certifications
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Our Factory

Since the establishment of the first production line in 1999, it has worked in the field of resin chemical industry for more than 20 years. At present At the same time, more than 5,000 tons of new pesticide intermediates can be produced each year. At the same time, the company has advanced laboratories and cooperates with major universities to continue to invest in new materials and new technologies.

 

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FAQ

Q: What is the difference between prepreg and epoxy?

A: "Prepreg" is the common term for a reinforcing fabric which has been pre-impregnated with a resin system. This resin system (typically epoxy) already includes the proper curing agent. As a result, the prepreg is ready to lay into the mold without the addition of any more resin.

Q: How long does prepreg take to cure?

A: Composites made with 3M™ Prepreg 3832 can be cured at temperatures from 250°F to 300°F depending on the service requirements. Recommended cure cycle: Apply 22 inches of mercury (minimum) vacuum and 85 psi pressure, ramp to 260°F at 10 ± 5°F per minute followed by a 2 hour hold at 260°F.

Q: How will humidity affect the curing of prepregs?

A: Exposure to moisture affects both how quickly thawed prepreg chemically ages and how it performs during cure [1,2]. There is at present no simple, reliable, production-floor test to determine how much a prepreg sheet may have degraded due to temperature and moisture exposure.

Q: What resin is used in prepreg?

A: Epoxy resins
The majority of aramid fiber prepregs use epoxy resins which require high-temperature/pressure cycles to flow, consolidate, and cure. This is usually done in an autoclave process. However, prepregs with other classes of resins, e.g., bismaleimides and polyesters, are made for special purposes.

Q: What temperature does carbon fiber epoxy cure at?

A: Around 100°C
Because curing will take place at around 100°C it is very important to use a release agent that will be effective at this temperature.

Q: What temperature should prepreg be stored at?

A: Storage of prepreg and b-stage materials in climate-controlled conditions is always preferred. Minimum Recommended Transportation and Storage Conditions: It is recommended that prepreg and b-stage materials be transported and stored in conditions where the 24-hour average temperature does not exceed 75°F (24°C).

Q: Does high humidity affect epoxy curing?

A: In addition, the moisture in the air can also cause the epoxy to foam or cause an extreme reaction and cure too quickly. Suggested humidity levels should be below 85%, ideally between 50-60%, throughout the full cure cycle, and the suggested temperature range for curing epoxy is between 70-80F.

Q: Why epoxy resin is used in composites?

A: Advantages of Epoxy Composites
In applications where minimizing weight is important, their excellent strength-to-weight ratio makes them ideal. They are also known for their corrosion resistance, design flexibility, and durability. In addition, epoxy composites provide various environmental benefits.

Q: How should prepregs be stored?

A: Prepreg will remain chemically within shelf life for up to 18 months at -18 °C. When not being used prepreg should be stored at -5°C or below to maximize shelf life. In frozen storage the Prepreg should be tightly sealed in its plastic sleeve and in the original box or stillage.

Q: What is the typical storage life for prepreg material?

A: For prepreg materials a general shelf life is first a year. After a year or after initial expiration some fabrics and prepregs may be re-tested for performance against its original stated performance specifications and bonding characteristics.

Q: What is the difference between prepreg and wet carbon fiber?

A: Prepreg carbon fiber has several advantages over wet carbon fiber, such as: Higher fiber-to-resin ratio, resulting in better mechanical properties and lighter weight. Better control over resin content and distribution, resulting in consistent quality and performance.

Q: What is the prepreg layup process?

A: The prepreg layup process involves placing layers of resin-impregnated reinforcement or other reinforcement materials in a precise position by hand. Workers manually manipulate individual plies and place them in position on a mold leaving no air pockets between each layer.

Q: What resin is used in prepreg?

A: Epoxy resins
The majority of aramid fiber prepregs use epoxy resins which require high-temperature/pressure cycles to flow, consolidate, and cure. This is usually done in an autoclave process. However, prepregs with other classes of resins, e.g., bismaleimides and polyesters, are made for special purposes.

Q: What are main advantages of using prepregs?

A: The major advantages of using prepregs are listed below:
Ease of use.
Low void content.
Good fatigue resistance.
Control of laminate thickness.
Good environmental and corrosion resistance.
Control of fibre volume fraction.
Clean process.
Better conformity and quality.

Q: What is the production method of prepreg?

A: In the hot melt prepreg method, the resin film is cast on a fibre-based carrier material, before both materials are passed between heated rollers. This transfers the resin to the carrier material and forces the resin to impregnate the carrier's fibres.

Q: Which manufacturing techniques use the prepreg as the feedstock material?

A: Prepreg is the starting material in the manufacturing of most composite aircraft structures although there is an increased interest in resin infusion and other non-prepreg processes.

Q: What is the resin in prepreg?

A: Many prepregs are based on epoxy or phenolic resin, but many thermosets may be used including high-tech materials like polyimide.

Q: Where is prepreg used?

A: Carbon fiber prepregs have been used in the airfoils of the Airbus fleet for more than 20 years. The usage of prepreg in automotive industry is used at relatively limited quantities in comparison with other techniques like automated tape lay-up and automated fiber placement.

Q: What are the characteristics of prepreg?

A: Basic prepreg selection is based on characteristics such as fiber, tow size, and weave selection, all of which are similar features to that of traditional fabrics. Prepregs will often come with a defined “cured ply thickness” and density in addition to providing the precise fiber to resin ratio.

Q: What are the specifications of prepreg?

A: Composites made with 3M™ Prepreg 3832 can be cured at temperatures from 250°F to 300°F depending on the service requirements. Recommended cure cycle: Apply 22 inches of mercury (minimum) vacuum and 85 psi pressure, ramp to 260°F at 10 ± 5°F per minute followed by a 2 hour hold at 260°F.

We're professional epoxy prepreg manufacturers and suppliers in China, specialized in providing high quality products with low price. We warmly welcome you to buy customized epoxy prepreg made in China here from our factory.

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